{ "id": "cond-mat/0002224", "version": "v1", "published": "2000-02-15T11:50:41.000Z", "updated": "2000-02-15T11:50:41.000Z", "title": "Ice XII in its second regime of metastability", "authors": [ "Michael Marek Koza", "Helmut Schober", "Thomas Hansen", "Albert Toelle", "Franz Fujara" ], "comment": "3 Pages of RevTeX, 3 tables, 3 figures (submitted to Physical Review Letters)", "categories": [ "cond-mat.stat-mech" ], "abstract": "We present neutron powder diffraction results which give unambiguous evidence for the formation of the recently identified new crystalline ice phase[Lobban et al.,Nature, 391, 268, (1998)], labeled ice XII, at completely different conditions. Ice XII is produced here by compressing hexagonal ice I_h at T = 77, 100, 140 and 160 K up to 1.8 GPa. It can be maintained at ambient pressure in the temperature range 1.5 < T < 135 K. High resolution diffraction is carried out at T = 1.5 K and ambient pressure on ice XII and accurate structural properties are obtained from Rietveld refinement. At T = 140 and 160 K additionally ice III/IX is formed. The increasing amount of ice III/IX with increasing temperature gives an upper limit of T ~ 150 K for the successful formation of ice XII with the presented procedure.", "revisions": [ { "version": "v1", "updated": "2000-02-15T11:50:41.000Z" } ], "analyses": { "keywords": [ "second regime", "metastability", "ambient pressure", "neutron powder diffraction results", "ice iii/ix" ], "note": { "typesetting": "RevTeX", "pages": 3, "language": "en", "license": "arXiv", "status": "editable" } } }